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| This technology comprises a process for the rapid preparation of fluorinated alkyl thiocyanates in high yield without the use of flammable solvents, without need for subsequent distillation, and in sufficiently high purity to allow ready hydrogenolysis to the corresponding fluorinated alkyl thiols. This process converts fluorinated iodides to thiocyanates in the presence of a quaternary ammonium salt catalyst.details fluorinated alkyl thiocyanates corresponding iodides phase transfer catalysis catalyst quaternary ammonium phosphonium salt catalyzes replacement ion pairs aqueous nonaqueous phases Quaternary transferred reaction proceeds absence solvent anion negligible |
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